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Equipment The 36-100 mini fractional distillation system is designed for difficult separations for
samples in the 100-1000 ml range
The 36-100 mini fractional distillation system is designed for difficult separations for samples in the 100-1000 ml range
High EfficiencyThis mini distillation system has up to 200 theoretical plates at atmospheric pressure. The very high number of theoretical plates allows it to produce extremely high purity materials and making difficult separations on small sample sizes.
The key to getting a great separation on small samples is spinning band technology. The spinning band combines high efficiency with low “hold up”. Less than 0.1 ml of sample is “held up” in the distillation column. Since the column only holds a small amount of sample, it can distill small sample sizes and give a high degree of separation.
Customized for your Application
The 36-100 mini distillation system can be configured according to your needs. Automation, vacuum systems, fraction collectors and other accessories can be integrated into the mini distillation system as needed. The result is a distillation apparatus customized to your specific needs.
Easy to useThe distillation process is fully automated from beginning to end, minimizing the time needed to operate the equipment. Easy programming of parameters makes you feel like a distillation expert. Heating, collecting of distillate and shut down of equipment at completion are all done automatically. Optional control from a PC.
Common applications include:- Crude Oil Distillation
- Petroleum Distillation
- Biodiesel Distillation
- High Purity Fractional Distillation
- Essential Oil Purification
- Vacuum Distillation
- Research Applications
Feature | Specifications | Benefit |
---|---|---|
Distillation Column Diameter | 8 mm | Small Diameter Provides Maximum Separating Power |
Distillation Column Length | 90 cm Long | Column Provides Maximum Separation |
Distillation Column Jacket | Vacuum Jacket and Silvered “Mirror” | Prevents Heat Loss from Distillation Column (Adiabatic) |
Condenser | Jacket Style | High Surface Area for Efficient Condensing |
Secondary Condenser | Cools Distillate Further Before Going to Receiver | Distillate in Receiver is Close to Room Temperature |
Boiler Heater | Electrical | Clean, Safe Heating of Boiler |
Boiler Sizes | 100, 250, 500 and 1000 ml | Available in Glass for Easy Viewing of Sample |
Boiler Stirring | Standard | Promotes Even Boiling and Gentle Heat Transfer |
Spinning Band Types |
Teflon - Operates up to 225 °C Stainless Steel – Operates Above 225 °C |
High Efficiency and High Temperature Bands |
Maximum Theoretical Plates |
Teflon Spinning Band 200 Stainless Steel Spinning Band - 85 |
High Efficiency Separation Combined with Low “Hold Up” |
Condensing Bath |
Optional Circulating Bath: -20 to 100 °C |
Automatically Cools and Heats Condenser |
Fraction Collector | 8 Place is Standard | Automatically Collect Fractions According to Vapor Temperature |
Vacuum Operation |
Optional Vacuum System
|
Automatic Control of Vacuum Level. Vacuum Reduces Boiling Points. Ideal for Thermally Sensitive Samples or High Boiling Materials |
Automatic Controller | Provides Automatic Control of the Entire Distillation Process | Start the Distillation and Walk Away |
PC |
Optional: Control From PC |
Perform a Distillation from a PC Analyze Distillation Results using our “Data View” Program. |
Safety Marks |
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Safe for Laboratory Use |
Power (Distillation Unit Only) |
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Configured for Local Power Requirements and with Local Power Plug, 115 or 220 V, 50/60Hz |
Other Utilities Required | Cooling Water or Circulating Bath | For Condenser |
Feature | Pilot Scale SPC | Lab Scale Distillation (9600) | Mini Distillation (36-100) | Micro Distillation (800) |
---|---|---|---|---|
Distillation Column Diameter | 50-150 mm | 21 mm | 8 mm | 7 mm |
Distillation Column Length (Standard) | 110 cm | 90 cm | 90 cm | 20 cm |
Maximum Theoretical Plates (Spinning Band Type) |
15, 30 or 45 |
Teflon 50 Stainless Steel 15 |
Teflon 200 Stainless Steel 85 |
Teflon 30 Stainless Steel 15 |
Boiler Sizes | 50 to 1000 liters |
Teflon 50 Stainless Steel 15 |
Teflon 200 Stainless Steel 85 |
Teflon 30 Stainless Steel 15 |
Boiler Sizes | 50 to 1000 liters | 1 to 50 liters | 100 to 1000 ml | 10 to 100 ml |
Material of Construction | Stainless Steel | Glass and Teflon | Glass and Teflon | Glass and Teflon |
Batch Distillation | Yes | Yes | Yes | Yes |
Automatic Control | Yes | Yes | Yes | Yes |