〈    Fractional Distillation
Mini Distillation
Equipment
The 36-100 mini fractional distillation system is designed for difficult separations for
samples in the 100-1000 ml range

Description
Specifications
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The 36-100 mini fractional distillation system is designed for difficult separations for samples in the 100-1000 ml range

High Efficiency

This mini distillation system has up to 200 theoretical plates at atmospheric pressure. The very high number of theoretical plates allows it to produce extremely high purity materials and making difficult separations on small sample sizes.

How Does it Work?

The key to getting a great separation on small samples is spinning band technology. The spinning band combines high efficiency with low “hold up”. Less than 0.1 ml of sample is “held up” in the distillation column. Since the column only holds a small amount of sample, it can distill small sample sizes and give a high degree of separation.



Customized for your Application

The 36-100 mini distillation system can be configured according to your needs. Automation, vacuum systems, fraction collectors and other accessories can be integrated into the mini distillation system as needed. The result is a distillation apparatus customized to your specific needs.

Easy to use

The distillation process is fully automated from beginning to end, minimizing the time needed to operate the equipment. Easy programming of parameters makes you feel like a distillation expert. Heating, collecting of distillate and shut down of equipment at completion are all done automatically. Optional control from a PC.

Common applications include:
  • Crude Oil Distillation
  • Petroleum Distillation
  • Biodiesel Distillation
  • High Purity Fractional Distillation
  • Essential Oil Purification
  • Vacuum Distillation
  • Research Applications
Feature Specifications Benefit
Distillation Column Diameter 8 mm Small Diameter Provides Maximum Separating Power
Distillation Column Length 90 cm Long Column Provides Maximum Separation
Distillation Column Jacket Vacuum Jacket and Silvered “Mirror” Prevents Heat Loss from Distillation Column (Adiabatic)
Condenser Jacket Style High Surface Area for Efficient Condensing
Secondary Condenser Cools Distillate Further Before Going to Receiver Distillate in Receiver is Close to Room Temperature
Boiler Heater Electrical Clean, Safe Heating of Boiler
Boiler Sizes 100, 250, 500 and 1000 ml Available in Glass for Easy Viewing of Sample
Boiler Stirring Standard Promotes Even Boiling and Gentle Heat Transfer
Spinning Band Types Teflon - Operates up to 225 °C

Stainless Steel – Operates Above 225 °C
High Efficiency and High Temperature Bands
Maximum Theoretical Plates Teflon Spinning Band 200

Stainless Steel Spinning Band - 85
High Efficiency Separation Combined with Low “Hold Up”
Condensing Bath Optional Circulating Bath:

-20 to 100 °C
Automatically Cools and Heats Condenser
Fraction Collector 8 Place is Standard Automatically Collect Fractions According to Vapor Temperature
Vacuum Operation Optional Vacuum System
  • 100-1 mmHg Range
  • Other Ranges Available
Automatic Control of Vacuum Level. Vacuum Reduces Boiling Points. Ideal for Thermally Sensitive Samples or High Boiling Materials
Automatic Controller Provides Automatic Control of the Entire Distillation Process Start the Distillation and Walk Away
PC Optional:

Control From PC
Perform a Distillation from a PC Analyze Distillation Results using our “Data View” Program.
Safety Marks
  • CE Marked
  • C TICK (Australia/NZ)
Safe for Laboratory Use
Power (Distillation Unit Only)
  • 115 V, 15 amps
  • 220 V, 8 amps
Configured for Local Power Requirements and with Local Power Plug, 115 or 220 V, 50/60Hz
Other Utilities Required Cooling Water or Circulating Bath For Condenser
Feature Pilot Scale SPC Lab Scale Distillation (9600) Mini Distillation (36-100) Micro Distillation (800)
Distillation Column Diameter 50-150 mm 21 mm 8 mm 7 mm
Distillation Column Length (Standard) 110 cm 90 cm 90 cm 20 cm
Maximum Theoretical Plates
(Spinning Band Type)
15, 30 or 45 Teflon 50
Stainless Steel 15
Teflon 200
Stainless Steel 85
Teflon 30
Stainless Steel 15
Boiler Sizes 50 to 1000 liters Teflon 50
Stainless Steel 15
Teflon 200
Stainless Steel 85
Teflon 30
Stainless Steel 15
Boiler Sizes 50 to 1000 liters 1 to 50 liters 100 to 1000 ml 10 to 100 ml
Material of Construction Stainless Steel Glass and Teflon Glass and Teflon Glass and Teflon
Batch Distillation Yes Yes Yes Yes
Automatic Control Yes Yes Yes Yes
Models
Pilot Scale
50-1000 liters
Lab Scale
1-50 liters
Mini Distillation
100-1000 ml
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