Welcome to B/R Instruments
Equipment The 800 micro fractional distillation system is designed for challenging separations for
the smallest of samples (7-100 ml).
The 800 micro fractional distillation system is designed for challenging separations for the smallest of samples (7-100 ml).
High EfficiencyThis micro distillation system has up to 30 theoretical plates at atmospheric pressure. It ideal for producing high purity materials and making difficult separations on very small samples.
How Does it Work?The key to getting a great separation on micro samples is spinning band technology. The spinning band combines high efficiency distillation with low “hold up”. Less than 0.1 ml of sample is “held up” in the distillation column. The micro spinning band distill tiny samples because only 0.1 ml of sample is actually in the distillation column at any time.
Customized for your ApplicationThe 800 micro distillation system can be configured according to your needs. Automation, vacuum systems, fraction collectors and other accessories can be integrated into the micro distillation system as needed. The result is a distillation apparatus customized to your specific needs.
Easy to useThe micro distillation process is fully automated from beginning to end, minimizing the time needed to operate the equipment. Easy programming of parameters makes you feel like a distillation expert. Heating, collecting of distillate and shut down of equipment at completion are all done automatically. Optional control from a PC.
Common applications include:- Crude Oil Distillation
- Petroleum Distillation
- Biodiesel Distillation
- High Purity Fractional Distillation
- Essential Oil Purification
- Vacuum Distillation
- Research Applications
Feature | Specifications | Benefit |
---|---|---|
Distillation Column Diameter | 7 mm | Small Diameter Provides Maximum Separating Power |
Distillation Column Length | 20 cm Long | Long Column Provides Maximum Separation |
Distillation Column Jacket | Vacuum Jacket and Silvered “Mirror” | Prevents Heat Loss from Distillation Column (Adiabatic) |
Condenser | Jacket Style | High Surface Area for Efficient Condensing |
Secondary Condenser | Cools Distillate Further Before Going to Receiver | Distillate in Receiver is Close to Room Temperature |
Boiler Heater | Electrical | Clean, Safe Heating of Boiler |
Boiler Sizes | 10, 15, 25, 50 and 100 ml | Available in Glass for Easy Viewing of Sample |
Spinning Band Types |
Teflon - Operates up to 225 °C Stainless Steel – Operates Above 225 °C |
High Efficiency and High Temperature Bands |
Maximum Theoretical Plates |
Teflon Spinning Band – 30 Stainless Steel Spinning Band - 15 |
High Efficiency Separation Combined with Low “Hold Up” |
Condensing Bath |
Optional Circulating Bath -20 to 100 °C |
Automatically Cools and Heats Condenser |
Fraction Collector | 8 Place is Standard | Automatically Collect Fractions According to Vapor Temperature |
Vacuum Operation |
Optional Vacuum System
|
Automatic Control of Vacuum Level. Vacuum Reduces Boiling Points. Ideal for Thermally Sensitive Samples or High Boiling Materials |
Automatic Controller | Provides Automatic Control of the Entire Distillation Process | Start the Distillation and Walk Away |
PC | Optional Control From PC | Perform a Distillation from a PC Analyze Distillation Results using our “Data View” Program. |
Safety Marks |
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Safe for Laboratory Use |
Power (Distillation Unit Only) |
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Configured for Local Power Requirements and with Local Power Plug, 115 or 220 V, 50/60Hz |
Other Utilities Required | Cooling Water or Circulating Bath | For Condenser |
Feature | Pilot Scale SPC | Lab Scale Distillation (9600) | Mini Distillation (36-100) | Micro Distillation (800) |
---|---|---|---|---|
Distillation Column Diameter | 50-150 mm | 21 mm | 8 mm | 7 mm |
Distillation Column Length (Standard) | 110 cm | 90 cm | 90 cm | 20 cm |
Maximum Theoretical Plates (Spinning Band Type) |
15, 30 or 45 |
Teflon 50 Stainless Steel 15 |
Teflon 200 Stainless Steel 85 |
Teflon 30 Stainless Steel 15 |
Boiler Sizes | 50 to 1000 liters |
Teflon 50 Stainless Steel 15 |
Teflon 200 Stainless Steel 85 |
Teflon 30 Stainless Steel 15 |
Boiler Sizes | 50 to 1000 liters | 1 to 50 liters | 100 to 1000 ml | 10 to 100 ml |
Material of Construction | Stainless Steel | Glass and Teflon | Glass and Teflon | Glass and Teflon |
Batch Distillation | Yes | Yes | Yes | Yes |
Automatic Control | Yes | Yes | Yes | Yes |