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〈    Fractional Distillation
Lab Scale Distillation
Equipment
The very efficient distillation column is well suited for producing high
purity materials and making difficult separations.

Description
Specifications
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Specifications for 9600 lab scale fractional distillation by B/R Instrument. Distill samples from 1 to 50 liters

High Efficiency

These lab scale fractional distillation systems have up to 50 theoretical plates at atmospheric pressure. The very efficient distillation column is well suited for producing high purity materials and making difficult separations.


Customized for your Application

The 9600 lab scale distillation system can be configured according to your needs. Automation, vacuum systems, fraction collectors and other accessories can be integrated into the distillation system as needed. The result is a distillation apparatus customized to your specific needs.

9600 Fractional Distillation


9600-50 Fractional Distillation

Easy to Use

The fractional distillation process is fully automated from beginning to end, minimizing the time needed to operate the equipment. Easy programming of parameters makes you feel like a distillation expert. Heating, collecting of distillate and shut down of equipment at completion are all done automatically. Optional control from a PC is available.


Common applications include:

  • High Purity Solvent Recycling
  • Petroleum Distillation
  • Biodiesel Distillation
  • Solvent Purification
  • High Purity Fractional Distillation
  • Essential Oil Purification
  • Vacuum Distillation
  • Crude Oil Distillation
Feature Specifications Benefit
Distillation Column Diameter 21 mm Large Diameter Provides Maximum Throughput
Distillation Column Length 90 cm Long Column Provides Maximum Separation
Distillation Column Jacket Vacuum Jacket and Silvered “Mirror” Prevents Heat Loss from Distillation Column (Adiabatic)
Condenser Inner Coil and Outer Jacket High Surface Area for Efficient Condensing
High Surface Area for Efficient Condensing Cools Distillate Further Before Going to Receiver Distillate in Receiver is Close to Room Temperature
Boiler Heater Electrical Clean, Safe Heating of Boiler
Boiler Sizes 1,2,3,5,12,22 and 50 liter sizes Available in Glass for Easy Viewing of Sample
Boiler Stirring Standard Promotes Even Boiling and Gentle Heat Transfer
Spinning Band Types Teflon - Operates up to 225 °C
Stainless Steel – Operates Above 225 °C
High Efficiency and High Temperature Bands
Maximum Theoretical Plates Teflon Band – 50
Stainless Steel - 20
High Efficiency Separation Combined with Low “Hold Up”
Condensing Bath Optional Circulating Bath
  • Optional Bath 1 0- 40 C
  • Optional Bath 2 -20 to 100 C
Automatically Cools and Heats Condenser
Fraction Collector Standard: 2 Place
Optional: 4 Place or 8 Place
Automatically Collect Fractions According to Vapor Temperature
Vacuum Operation Optional Vacuum System
  • 100-1 mmHg Range
  • Other Ranges Available
Automatic Control of Vacuum Level. Vacuum Reduces Boiling Points. Ideal for Thermally Sensitive Samples or High Boiling Materials
Automatic Controller Provides Automatic Control of the Entire Distillation Process Start the Distillation and Walk Away
PC Optional Control From PC Perform a Distillation from a PC Analyze Distillation Results using our “Data View” Program.
Safety Marks
  • CE Marked
  • Listed to UL 6101.1 by ETL
  • Listed to CSA C22.2 1010.1 by ETL
  • C TICK (Australia/NZ)
Safe for Laboratory Use
Power (Distillation Unit Only)
  • 1-22 liter (115 V) 15 amps
  • 1-22 liter (220 V) 8 amps
  • 50 liter (220V) 15 amps
Configured for Local Power Requirements and with Local Power Plug, 115 or 220 V, 50/60Hz
Other Utilities Required Cooling Water or Circulating Bath For Condenser
Feature Pilot Scale SPC Lab Scale Distillation (9600) Mini Distillation (36-100) Micro Distillation (800)
Distillation Column Diameter 50-150 mm 21 mm 8 mm 7 mm
Distillation Column Length (Standard) 110 cm 90 cm 90 cm 20 cm
Maximum Theoretical Plates
(Spinning Band Type)
15, 30 or 45 Teflon 50
Stainless Steel 15
Teflon 200
Stainless Steel 85
Teflon 30
Stainless Steel 15
Boiler Sizes 50 to 1000 liters Teflon 50
Stainless Steel 15
Teflon 200
Stainless Steel 85
Teflon 30
Stainless Steel 15
Boiler Sizes 50 to 1000 liters 1 to 50 liters 100 to 1000 ml 10 to 100 ml
Material of Construction Stainless Steel Glass and Teflon Glass and Teflon Glass and Teflon
Batch Distillation Yes Yes Yes Yes
Automatic Control Yes Yes Yes Yes
9600 Spinning Band Distillation
Models
Pilot Scale
50-1000 liters
Lab Scale
1-50 liters
Mini Distillation
100-1000 ml
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