Vacuum Distillation
The manually operated ASTM D1160 vacuum distillation system is a turnkey system including everything needed to perform a D1160 distillation.
- Adjust manual control valve to obtain the desired vacuum level
- Adjust the heat control to obtain the desired distillation rate
- Set the desired condenser and receiver temperature on the circulating bath
- Record the first drop
- Record the vapor and boiling flask temperature at receiver volumes of 5%, 10%, 20% …. 90%, 95% and at the final boiling point (FBP)
New and experienced operators will find this system simple to use. The turn key system is easy to use with only 3 settings for the operator to control. Easy access to all the distillation components makes performing the test as simple as possible.
- Distillation rate adjusted with manual heat control
- Vacuum level adjusted with manual control valve
- Receiver/condenser temperatures set on bath
Operator manually records
- First drop (IBP)
- Vapor temperature, pot temperature, vacuum level and distillation rate at 5%, 10%, 20%....volume and final boiling point (FBP)
Boiling Flask/Heating Mantle
- 500 ml
- Borosilicate or quartz
- High wattage heating mantle
- Insulating top
Distillation Column
- According ASTM specifications
- Vertical viewing window for easy viewing
- Highly reflective vacuum jacket
- Adjustable vapor temperature probe
First Drop Detector
- Automatically detects and records the first drop (IBP)
Receiver/Volume Measurement
- Programmable receiver temperature
- Programmable
- 30-100°C Standard
- Optional -10 to 100 °C
- Low liquid cut off
- Over temperature cut off
Vacuum Operation
- Manually operated control valve
Vacuum Components
- 100-1 mmHg range standard (MKS)
- Optional 760-100 mmHg range (MKS)
- Optional 1-0.1 mmHg range (MKS)
- Control valve (MKS)
- Vacuum pump (Edwards)
Cold Trap
- Cooling by dry ice
- Optional automatic cooler, -60 °C
- Graduated
- Easy access
- Easy to see contents
- Easy to remove contents
Dimensions
- 91.5 cm x 94 cm x 53 cm (H x W x D)
Power (Distillation Unit Only)
- 10 amps 220 VAC
| Fully Automatic | Semi-Automatic | Manually Operated | |
|---|---|---|---|
| Digital Temperature and Vacuum Display | |||
| Vacuum Control | |||
| Distillation Rate | |||
| Volume Measurement | |||
| Condenser/Receiver Temperature | |||
| Shut Down on Test Completion | |||
| Control and Test Report from PC |
There are so many reasons to choose a B/R D1160. Here are a few.
Complete System Includes:
Includes everything needed to perform the D1160 test
Easy to operate
Digital temperature and vacuum readouts makes controlling the unit easy. Just set the vacuum level, condenser temperature and adjust the boiling flask heat. It's that simple.
Upgradeable
Upgrade to fully-auto D1160.
The semi-automatic D1160 can be upgraded in the field to the fully automatic. The D1160 can change, as your needs change.
distillation equipment since 1966.
