B/R Instruments | 9600 High Efficiency Distillation System

Applications 9600 High Efficiency Distillation System The 9600 spinning band distillation system is used for high purity applications

This high efficiency, fractional distillation system is an ideal tool for automatically purifying or analyzing a wide range of materials. Common applications include:

High Purity Solvent Recycling
GPC Solvent Recycling
General Lab Solvent Recycling
Petroleum Distillation
Biodiesel Purification
Crude Oil Distillation
Solvent Purification
Essential Oil Purification
Vacuum Distillation

This high efficiency distillation system can be equipped with two different types of distillation columns, spinning band columns and packed columns.

The 9600 spinning band distillation system is used for high purity applications and features:

All Glass and Teflon Components
50 Theoretical Plate Distillation Column
1 to 50 liter boiler capacities
Automatic and Manually Operated Distillation Systems

Column Specifications

Column	Length	Diameter	Plates	Flask Sizes
9600 Spinning Band	90 cm	21 mm	50 (Teflon Band)	1, 5, 12, 22 and 50 liter

The 9600 packed column distillation system for large boilers and high throughputs features:

15-20 Theoretical Plate Distillation Column
1 to 50 liter boiler capacities
A variety of packing materials
Automatic and Manually Operated Distillation Systems

9600 30 Plate Fractional Distillation Apparatus

Traditional packed distillation columns are used for applications that require high distillation rates or that require boiler sizes larger than 50 liters. A variety of distillation column packing types are available including various random and structured packing. Packing materials can be made of metal, ceramic or glass.

Column Specifications

Column	Diameter	Plates	Boiler Sizes
9600 Packed	25 to 150 mm	15-30	1 to 500 liters

Automatic Controller (Optional PC Interface)

The automatic controller minimizes the amount of operator time required for each distillation. Select your stored distillation program and let the controller perform the distillation. Collect up to 8 fractions. Each fraction has programmable:

Open Temperature
Close Temperature
Heat Rate
Reflux Ratio
Programmable shut down at end of distillation

Each distillation program has a programmable:

Vacuum level
Maximum Boiler temperature (safety feature)
Equilibration Time

The controller allows easy editing of parameters while the distillation is in progress. Or run the distillation from a PC.

Optional Accessories

Automatic Fraction Collector
Automatic Vacuum Control
Heating/Cooling Bath
PC Control
Many Other Option

Vacuum Regulation System

Materials that have very high boiling points or are subject to thermal degradation should be distilled at reduced pressures. The VAC-1000 is a complete, stand alone, vacuum system that can provide regulated vacuum to any distillation system. It features a 5 decade pressure sensor, control valve, cold trap, vacuum pump, all mounted on a roll around cart for easy maneuverability in the laboratory.

Automatic Fraction Collectors

Two, four and 8 place fraction collectors are available to direct distilled material to the desired receiver. Automated versions allow distilled fractions to be collected unattended. Various size receivers are available in glass, stainless steel and plastic.

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